酷玩手游

                                                                                                                                                □ 王乐新 王云

     KAER·FEIXIUKULUNFAWEILIANGSHUIFENCEDINGYIGUANGFANYINGYONGYUCEDINGSHIYOU、HUAGONG、QINGGONG、DIANLI、YIYAO、NONGYAO、HUANBAO、DIZHI、SHIPINDENGXINGYECHANPINZHONGDESHUIFENHANLIANG。YOUYUJINNIANGEDANWEIDUICHANPINZHILIANGDEZHONGSHI，DUIGAIZHONGYIQIDEYINGYONGZHUNIANZENGJIA，YINCIZHIDINGGAIZHONGYIQIDEJIANDINGGUICHENGJIUXIANDEYOUWEIPOQIEHEZHONGYAO。JINGGUONULI，JJG1044-2008《KAER·FEIXIUKULUNFAWEILIANGSHUIFENCEDINGYI》JIANDINGGUICHENGYU2008NIAN9YUE27RIJINGGUOJIAZHIJIANZONGJUPIZHUNFABU，BINGZI2009NIAN1YUE1RIQISHIXING。

       GUICHENGFABUSHISHIHOU，QUANGUODEZIXUNDIANHUABUSHAO。YOUYUGAIZHONGYIQICAOZUOJIAOWEIJIANDAN，GUICHENGZHONGDEJIANDINGFANGFABIJIAOXIANGXI，YINCIZIXUNYIQIJIANDINGFANGFADEJIAOSHAO， ERZIXUNBIAOZHUNWUZHIXIANGGUANWENTIDEJIAODUO。ZAIXIEGAIGUICHENGSHI，YIQICEDINGDIHANSHUILIANGZHIDEJIANDING，XUYAOYOUGUOJIABIAOZHUNWUZHIDEZHICHENG，DANGSHIGUOJIAJILIANGYUANYIYOUSHUI-JIACHUNBIAOZHUNWUZHI，SHUIHANLIANGWEI1mg/g，DANSHIYOUYUSHENGCHANLIANGHENSHAO，JINGCHANGMAIBUDAO。WODANWEIXIANZAIZHENGZAIYANZHIHESHENBAOSHUI-JIACHUNBIAOZHUNWUZHI， DANZHEIXUYAOYIGEBIJIAOZHANGDEGUOCHENG。BIAOZHUNSHUIRONGYEMAIBUDAO，DANJIANDINGSHUIFENCEDINGYIYOUBIXUYOUSHUI-JIACHUNBIAOZHUNRONGYECAIXING，ZENMEBAN？ MUQIANZHUANGKUANGXIA，ZHINENGZIJIPEIZHI。ZAIKONGZHIHAOBUQUEDINGDUDEQIANTIXIA，SHIKEYIZIJIPEIZHISHUI-JIACHUNBIAOZHUNRONGYEDE。XIAMIANJIUGUICHENGQICAOZHONGSUOYUDAODEYIXIEWENTIHEXIANGFA、GUICHENGDESHIYONGFANWEI、ZAIYIQIJIANDINGZHONGDEZHUYISHIXIANGHEBIAOZHUNWUZHIDEPEIZHIFANGFADENGZUORUXIASHUOMING。

一、关于规程的名称及适用范围的说明

GUANYUGUICHENGDEMINGCHENG，WEISHENMEBUCHENGZHIWEI《WEILIANGSHUIFENCEDINGYI》JIANDINGGUICHENG， ERBIXUXIANDINGZAIKAER·FEIXIUKULUNFAWEILIANGSHUIFENCEDINGYIDEFANWEI？JULEJIE，WEILIANGSHUIFENCEDINGYIDEZHONGLEIMUQIANANFENXIFANGFADAZHIFENWEIHONGGANFASHUIFENCEDINGYI、DIANZU（DIANDAO）FASHUIFENCEDINGYI、KAER·FEIXIUTIJI（DIDING）FASHUIFENCEDINGYI、KAER·FEIXIUKULUNFASHUIFENCEDINGYISIDALEI。QIANLIANGZHONGYIYOUGUOJIAJILIANGJIANDINGGUICHENG，CICIBIANXIEGUICHENGKAISHIXIANGBAKASHITIJI（DIDING）FAHEKASHIKULUNFADOUXIERUGUICHENG，DANHOULAIFAXIANKASHIDIDINGFADEYIQIZHONGLEIJIAODUO，JISHUZHIBIAOCHABIEYOUTAIDA，ZHIYOUJINKOUDESHUZIDIDINGSHIYIQIHEKULUNFAYIQIJISHUZHIBIAOJIEJIN。BIZHEZAIDUONIANDEYIQIJIANXIAOGUOCHENGZHONGFAXIAN，GUOCHANSHUZITIJI（DIDING）SHISHUIFENYIYOUYUJINGMIJIAGONGJISHUJIAOCHA，HUOSHICAILIAONAIMOXINGJIAOCHADENGYUANYIN，YIQICHUCHANGSHIJISHUZHIBIAOHAIKEYI，DANSHIYONGJINIANHOU，YOUYUMOSUN、MIFENGJISHUJIAOCHAHUOJIXIECHUANDONGHUICHAJIAODA，JISHUZHIBIAOXIAJIANGHENDUO，BATAMENXIANDINGZAIYIGEGUICHENGZHONG，JIANGHUIZAOCHENGHENDUOYIQIBUHEGE。CIWAI，KASHISHOUDONGTIJI（DIDING）SHISHUIFENCEDINGYICELIANGFANWEIZHAI、ZHUNQUEDUDI，RUOYAOTUOKUANCELIANGFANWEI、TIGAOZHUNQUEDU，ZHENDUIBUTONGDEJIANDINGJIUBIXUPEIZHIBUTONGDIDINGDUDEDIDINGYEDUOZHONG，DANDUIDIDINGYEDEBUQUEDINGDUJINXINGFENXIYOUCHENGWENTI， BINGQIEDIDINGYEBUYICUNFANG，DIDINGDURONGYIGAIBIAN。SUOYI，ZUIHOUMEIYOUBA“TIJI（DIDING）SHIWEILIANGSHUIFENCEDINGYI”XIERUGUICHENGZHONG。ER“SHUZITIJI（DIDING）SHIWEILIANGSHUIFENCEDINGYI”KEYICANZHAOBENGUICHENGZHIXING（JISHUZHIBIAOXIANGJIN）。

    二、规程的试验情况

ZAIGUICHENGQICAOGUOCHENGZHONG， WOMENTONGGUOHESHENGCHANCHANGJIAHEZUODEFANGSHI， DUIKAER·FEIXIUKULUNFAWEILIANGSHUIFENCEDINGYIJINXINGLEDALIANGDESHIJIJIANCE，WEIBIANXIEGUICHENGJILEILEDIYISHOUJISHUSHUJU。WEILIANGSHUIFENCEDINGYIDEXIAOZHUNGONGZUOZAIWOYUANYIKAIZHANDUONIAN，GUOQUWOMENZAISHUIFENYIDEJIANCEZHONG，DADUOCAIYONGXIANGDUISHIZHIWUCHAFANGSHI。ZAIGUICHENGBIANXIECHUQIYEXIANGCAIYONGXIANGDUISHIZHIWUCHADECELIANGFANGSHI，DANWOYUANXIAOZHUNGUIFANYAOQIUXIAOZHUNDESHUIFENHANLIANGJIAODA，ZAI（500～5000）μgFANWEINEI，YONGCHUNSHUICELIANGYIQIDEXIANGDUISHIZHIWUCHASHIKEXINGDE。DANSHISHUIFENZAI500μgYIXIAFANWEIDECELIANG，ZAISHIJIYINGYONGZHONGSHIZUIDUODE，ZHEIGEFANWEINEIDEZHUNQUEYUFOUSHIFEICHANGZHONGYAODE，ZHEIYESHIBIANXIEGUOJIAJILIANGJIANDINGGUICHENGDEZHUYAOMUDE。YINCI，GUICHENGZHONGBIXUBAOHANJIWEILIANGSHUIFENDUAN。DANGSHUIFENWEI10μg

SHI，ZAIJINCHUNSHUIYIJINGBUXINGLE，JISHIJINSHUI-JIACHUNBIAOZHUNRONGYE，QIYIQIDEXIANGDUISHIZHIWUCHAYETAIDA，DADAO30％YISHANG，WOMENBASHIZHIWUCHA30％YISHANGDEYIQIPANDINGWEIHEGEXIANRANSHIBUHESHIDE。NEIME，SHIFOUKEJIANG10μgDIANDINGWEIJUEDUIWUCHA，QITAJIANDINGDIANDINGWEIXIANGDUIWUCHA？ SHIZHIWUCHAPINGDINGBIAOZHUNJIBUTONGYI，BUQUEDINGDUFENXIYOUBUHAOPINGDING，ZUIHOUHAISHIJIANGSHIZHIWUCHATONGYICAIYONG±（5%JIANDINGDIAN+3）μgLAIPINGDING， ZHEIYEFUHEYIQICELIANGFANWEINEIDEWUCHAXIANXINGFENBUTEXING。

    三、测量为何不取范围而取检定点

ZAIQITAGUICHENGZHONGDADUOQUJIANDINGCELIANGFANWEIERBUSHIJIANDINGDIAN。QIEQUCELIANGFANWEIDEGUICHENG，JIANDINGYONGBIAOZHUNWUZHIDEHANLIANGDADUOSHIBULIANXUDE，ERSHUIFENCEDINGYIDESHUIHANLIANGJIANDINGYONGBIAOZHUNWUZHISHILIANXUDE。ZHEIJIURONGYIDUITONGYITAIYIQIDAILAIBUTONGDEPINGJIAJIEGUO。BIRUYOUYITAIZAI10μgDIANBUHEGE，DANZAI100μgDIANQUEHEGEDEYIQI，DANGBASHIZHIWUCHADINGWEI（10~100）μgCESHUIFANWEISHI，JINYANGJIEJIN10μgDIANSHIPANDINGYIQIWEIBUHEGE；DANGJINYANGJIEJIN100μgDIANSHIPANDINGYIQIWEIHEGE，TONGYIFANWEI，TONGYITAIYIQIQUEYOUYUCELIANGFANGSHIBUTONGYIERDAILAIBUTONGDEPINGJIAJIEGUO，BUHAOJIEDING。XUANZEJIANDINGDIANWUCHAJIUCHANSHENGZAIZHEIGEDIANSHANG，ZHEIYANGJIAOKEXUE，BUHUIYINCELIANGFANGFABUTONGERDAOZHIYIQIHEGEHUOBUHEGEDEBUTONGJIEGUO，YINCI，ZUIHOUHAISHIQUEDINGYONGJIANDINGDIANLAIJIANDINGYIQIDESHIZHIWUCHA。

    四、标准物质为何选取甲醇-水

SUIYOUXUDUOSHUIHANLIANGBIAOZHUNWUZHI， DANJJG1044-2008CAIYONGSHUI-JIACHUNBIAOZHUNWUZHIZUOWEIJIANDINGYONGBIAOZHUNWUZHI。WEIHEBUCAIQUQITAGUTIBIAOWUHEYETIBIAOWUNI？ ZHUYAOYUANYINSHIGUTIWUZHIQUYANG、CHENGYANG、JINYANGGUOCHENGJIAOZHANG，BAOLUZAIKONGQIZHONGYIGAIBIANSHUIFENHANLIANG，JINYANGSHIHAIXUDAKAIDIANJIECHI，ZHISHIDIANJIECHIZHONGJINRUHANSHUIDEKONGQIERYINGXIANGCELIANGJIEGUO，QITARONGYEBIAOWUYOUYUNEIHANWUCHENGFENBUTONGKENENGYUDIANJIEYEFASHENGFANYING，ERSHUI-JIACHUNBIAOZHUNWUZHIZHONG，JIACHUNSHIDIANJIEYEDEZUCHENGBUFEN，SHUISHIBEICEBIAOWU，YOUYUCEDASHUILIANGZHISHIZHIJIEJINCHUNSHUI，ZHIYOUZAIWEISHUILIANGZHISHICAIJINSHUI-JIACHUNBIAOZHUNWUZHI，ZHEIYANGBIAOZHUNWUZHIBUZHIYUYINGXIANGDIANJIEYEDEPEIBIJILINGPINGHENGDIAN。SUOYI，CAIYONGSHUI-JIACHUNBIAOZHUNWUZHI。

    五、检定项目的设立及意义

1.SHIZHIWUCHA：JIANDINGYIQISHUIHANLIANGCELIANGJIEGUOSHIFOUZHUNQUE。

2.CELIANGZHONGFUXING：JIANDINGYIQIZAICELIANGXIANGTONGSHUIHANLIANGWUZHISHIDEZAIXIANXING。

3.DIANJIESUDU：JIANDINGYIQIDEFENXIXIAOLV。

4.LINGDIANPINGHENGSHIJIAN：JIANDINGYIQIMIFENGSHIFOUWANHAO、DIANJISHIFOUWURAN、DIANJIEYESHIFOUGUOQI、FANGDADIANLUSHIFOUWENDINGDENG。

5.JUEYUANDIANZU：JIANDINGYIQIDEANQUANXINGNENG。

6.JUEYUANQIANGDU：JIANDINGYIQIDEANQUANXINGNENG。

7.XIELOUDIANLIU：JIANDINGYIQIDEANQUANXINGNENG。

    六、检定中应注意的事项

WOMENZAIRICHANGJIANDINGZHONGFAXIAN，YONGCHENGZHONGJINYANGFAJIANDINGYIQIBIYONGTIJIJINYANGFACELIANGWUCHAYAOXIAO，DANJIAOWEIMAFAN。RUGUOJIANDINGYIQIHETIANPINGSHIJIAOJINHAIKEYI，DANRUGUOJIAOYUAN，JIANDINGJIUJIBUFANGBIAN。ERYONGTIJIJINYANGFAJIANDINGYIQIZAIDABUFENQINGKUANGXIASHIKEXINGDE（JINYANGQIWUCHAJIAODASHI、RENWEIJINYANGWUCHAJIAODASHIZEBUXING），DANGYIQIYONGTIJIJINYANGFAJIANDINGWEIHEGESHI，KEYIPANWEIHEGE。DANGYIQIJIANDINGWEIBUHEGESHI，ZAIJIANGYIQIBANDAOTIANPINGSHIFUJINJINXINGCHENGZHONGJINYANGLAIZUIZHONGPANDINGYIQISHIFOUHEGE。CIWAI，GUICHENGZHONGYOUYICHULURUXINGCUOWU，JIDIANJIESUDUDEJILIANGXINGNENGYAOQIUYINGWEI10min，YUGUICHENGFULUCHEDZHONGDEDIANJIESUDUDEJISHUYAOQIUXIANGYIZHI。

    七、水-甲醇标准溶液的配制

RUHEPEIZHISHUI-JIACHUNBIAOZHUNRONGYE？ XIEGUICHENGSHI，WEILEKAOXIANGYIYOUDESHUIBIAOZHUNWUZHI， ERCAIYONGDE1mg/gSHUI-JIACHUNBIAOZHUNWUZHI，1mg/gSHUIBIAOZHUNWUZHINENGYONG， DANBINGBUSHIJIANDINGSHUIFENCEDINGYIDEZUIJIAPEIBI，YINSHUIHANLIANGTAIDIJIYIXISHOUKONGQIZHONGDESHUIFEN，ERYINGXIANGCELIANGJIEGUO。ZUIJIAPEIBIWEI10mg/mL（HUO10mg/g）ZUOYOU。XIANDUIPEIZHIFANGFAJIZHUYISHIXIANGZUOJIAOWEIXIANGXIDESHUOMING。SUOXUSHEBEI：TIANPING：SHIWANFENZHIYI；TIJIDIDINGFASHUIFENCEDINGYI：JIANCEHEGE；JIACHUN：SEPUCHUN（YEXIANGSEPUYIYONGJIKE，ZUIHAOSHIXINDE，HANSHUILIANGDI）；RONGLIANGPING：AJIHEGE；WEILIANGJINYANGQI：JIANCEHEGE。

（1）SHOUXIANBIXUPEIZHIJIAODADELIANG，YINWEIJIACHUNYIXISHUI，JIACHUNLIANGSHAOXISHOUKONGQIZHONGDESHUIFENZHANBIJIAODA；BENDICELIANGSHISHUIFENHANLIANGBIANHUAJIAODA； CHENGLIANGTIANJIASHUIFENWUCHAJIAODA。RONGLIANGPINGZHISHAOYINGZAI100mLYISHANG。

（2）XUANQUSEPUCHUNJIACHUN，DAORUYIZHIZHONGLIANGDERONGLIANGPINGZHONG，YAOYUN。CHOUQU500μLZUOYOUJIACHUNCHENGZHONGHOUJINYANGDAOYIPINGHENGHAODETIJIDIDINGFASHUIFENCEDINGYIZHONG，ZAICHENGZHONG。LIANXUJINYANG6CI，SUANCHUJIACHUNZHONGDEBENDIHANSHUILIANG，CHENGLIANGZHUANGJIACHUNDERONGLIANGPINGZHONGLIANG，SUANCHUJIACHUNLIANG，ZAISUANCHUYINGTIANJIADECHUNSHUILIANG，YONGSHIYIDEJINYANGQICHOUSHUIZAITIANPINGCHENGLIANGHOUTIANJIA，DEDAO10mg/gDESHUI-JIACHUNRONGYE。

（3）XUANQUSEPUCHUNJIACHUN，DAORURONGLIANGPINGZHONG，YAOYUN。CHOUQU500μLZUOYOUJIACHUNCHENGZHONGHOUJINYANGDAOYIPINGHENGHAODETIJIDIDINGFASHUIFENCEDINGYIZHONG，ZAICHENGZHONG。LIANXUJINYANG6CI，SUANCHUJIACHUNZHONGDEBENDIHANSHUILIANG，ZAISUANCHUYINGTIANJIADECHUNSHUILIANG， JIANGCHUNSHUIZHURUZHUANGJIACHUNDERONGLIANGPINGZHONG，ZAIZHURUJIACHUNZHIKEXIAN，DEDAO10mg/mLDESHUI-JIACHUNRONGYE。

YISHANGLIANGZHONGPEIZHIFANGFA，QIANYIZHONGYINGXIANGYINSUJIAOXIAO，ZHIYUTIANPINGHETIJIDIDINGFASHUIFENCEDINGYIDEWUCHAYOUGUAN，HEJINYANGQI、RONGLIANGPINGWUGUAN，BUQUEDINGDUJIAOXIAO，ZHEIYESHIWOMENYINGYONGBIJIAOHAODEFANGFA。QUEDIANSHIPEIZHILIANGJIAOSHAO，SHOUKONGQIZHONGSHUIFENDEYINGXIANGJIAODA，ZUIHAOZAITIANQIGANZAOSHIPEIZHI。PEIZHICHENGZHILIANGBI，TIJIJINYANGSHIBIXUCHENGYI0.792MIDUXISHU， DANGRANYEKEYIYONG0.792MIDUXISHUHUANSUANPEIZHICHENG10mg/mLDESHUI-JIACHUNRONGYE，ZHEIZAITIJIJINYANGSHIJIAOWEIFANGBIAN。ZAIPEIZHIGUOCHENGZHONG，XUANZETIJIDIDINGFASHUIFENCEDINGYIDEYUANYINSHIYINWEICEDINGJIACHUNDEBENDIHANSHUILIANGSHI，BIXUJIADAJINYANGLIANG（YOUSHIXUJINmLJIDEJIACHUN）CAINENGZHUNQUECECHUBENDISHUIHANLIANG，ERKULUNFASHUIFENYIZAIDAJILIANGJIARUJIACHUNSHI，DIANJIEYEPEIBIFASHENGJIAODAGAIBIAN，RONGYIZAOCHENGCEDINGKAISHISHIDELINGDIANHECEDINGHOUDELINGDIANBUTONG，WUCHAYUECEYUEDA。ERTIJIDIDINGFASHUIFENCEDINGYIKAISHIDIDINGSHIYONGDEJIUSHICHUNJIACHUN，JIADAJINYANGLIANGYEBUHUICHUXIANCELIANGWUCHAZENGDADEQINGKUANG。YONGSHANGSHUFANGFACEDINGJIACHUNBENDISHUIFENSHI，DANGWENDINGCEDEYIGEZHISHI，YINGDANGZAIJIADAJINYANGLIANGCELIANG，YIYANZHENGBENDISHUIFENDECELIANGSHIFOUZHUNQUE；DANGJINGJISUANTIANJIASHUIFENHOUZAIJINXINGFANCE，TONGYANGKEYIYANZHENGYIQIDESHIZHIWUCHA，ZHEIZAIYIHOUDEBUQUEDINGDUJISUANZHONGYONGDAO。JINGDUIBUQUEDINGDUDEJISUAN，JIEGUOMANZUGUICHENG（U=1.4，k=2）DEYAOQIU。

ZUOZHEDANWEI【SHANDONGSHENGJILIANGKEXUEYANJIUYUAN】